Chemistry EEI Take
2
Theory: Investigating the extent to which like
dissolves like.
Investigate: How does the Ksp of salt in water
compare to the Ksp of salt in slightly polar and non-polar solutions.
1) Ksp of salt in water
2) Ksp of salt in ethanol
3) Ksp of salt in oil
Then investigate temperature dependence of the Ksp of salt
in the same solutions, at a constant temperature.
How do the results of this experiment contribute to the
theory ‘like dissolves like’?
General Equipment list/method:
bubette
retort stand
clamp
ethanol
oil
distilled water
Therefore, I need to investigate the cause of separation of
the Na ions from the Cl ions
Procedure:
1. Select “Hot Plate & Mag Stir” from
the Equipment menu. Place 25.00 mL of an
unknown brine solution into a 100 mL beaker.
Place the beaker on the magnetic stirrer. Add 0.100 mL of potassium chromate. Select
the magnetic stirrer and use the context menu to set the stirring rate.
2. Carefully fill a 50.00 mL burette with
standardized silver nitrate solution. Zero the burette to 0.00 mL and
position it over the 100 mL beaker.
3. Titrate the contents of the beaker with
silver nitrate from the burette.
Initially the silver nitrate may be added rapidly with continuous
stirring. At this point, large amounts
of white solid should be forming. Slow
down subsequent additions of silver nitrate until a faint brick red precipitate
forms indicating the end of the titration.
4.
Record all pertinent data on the data sheet. Read the burette volume to +/- 0.1 mL .
5.
Repeat the titration until the final volumes agree to
+/- 0.2 mL.
6.
Fill in the remainder of the data sheet and perform
all calculations.
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